rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea

Base Information

• Chemical Name: rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea
• CAS No.: 1417658-03-7
• Molecular Formula: C₁₄H₂₀N₄OS
• Molecular Weight: 292.405
• Mol file: 1417658-03-7.mol

Synonyms:rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea

Chemical Property of rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea

There total 1 articles about rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzylpyrrolidine-2-carbohydrazide (1401686-36-9) + methyl thioisocyanate (556-61-6) → rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea (1417658-03-7)

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.1002/hlca.201200400

Reference yield: 90.0%

rac-1-({[1-benzylpyrrolidine-2-yl]carbonyl}amino)-3-methylthiourea (1417658-03-7) → rac-5-[1-benzylpyrrolidin-2-yl]-N-methyl-1,3,4-thiadiazol-2-amine (1401686-35-8)

Guidance literature:

With sulfuric acid; at 20 ℃; for 24h;

DOI:10.1002/hlca.201200400

upstream raw materials:

1-benzylpyrrolidine-2-carbohydrazide

methyl thioisocyanate

Downstream raw materials:

rac-5-[1-benzylpyrrolidin-2-yl]-N-methyl-1,3,4-thiadiazol-2-amine