N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide

Base Information

Chemical Name:N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide
CAS No.:929903-76-4
Molecular Formula:C₂₀H₂₄BrNO₂Si
Molecular Weight:418.406
Hs Code.:

Synonyms:N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide

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Chemical Property of N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide

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Technology Process of N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide

There total 2 articles about N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5683-31-8
3-(trimethylsilyl)prop-2-ynoic acid

: 1245538-54-8
1-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-(methylamino)but-2-yn-1-ol hydrochloride

: 929903-76-4
N-{4-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-hydroxybut-2-yn-1-yl}-N-methyl-3-(trimethylsilyl)prop-2-ynamide

Guidance literature:: 3-(trimethylsilyl)prop-2-ynoic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; for 0.5h; Inert atmosphere;

1-[2-(2-bromoprop-2-en-1-yl)phenyl]-4-(methylamino)but-2-yn-1-ol hydrochloride; With triethylamine; In dichloromethane; N,N-dimethyl-formamide; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.051