C₂₇H₃₆N₄O₈SSi

Base Information

Chemical Name:C₂₇H₃₆N₄O₈SSi
CAS No.:1000612-07-6
Molecular Formula:C₂₇H₃₆N₄O₈SSi
Molecular Weight:604.756
Hs Code.:

C<sub>27</sub>H<sub>36</sub>N<sub>4</sub>O<sub>8</sub>SSi

Synonyms:C₂₇H₃₆N₄O₈SSi

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Chemical Property of C₂₇H₃₆N₄O₈SSi

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Technology Process of C₂₇H₃₆N₄O₈SSi

There total 7 articles about C₂₇H₃₆N₄O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1000612-04-3
C₁₆H₂₄N₂O₂Si

: 54145-10-7
ethyl N-<<(4-methylphenyl)sulphonyl>oxy>carbamate

: 1000612-07-6
C₂₇H₃₆N₄O₈SSi

Guidance literature:: With calcium oxide; In dichloromethane; at 15 ℃; for 18h;
DOI:10.1055/s-2007-986664

Reference yield:

: 1000612-01-0
C₁₆H₂₄Br₂N₂O₃Si

: 1000612-07-6
C₂₇H₃₆N₄O₈SSi

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / H₂; Et₃N / Pd/C / methanol; CH₂Cl₂ / 5 h / 20 °C

2: 84 percent / MsCl; DBU / 18 h / 0 °C

3: 50 percent / CaO / CH₂Cl₂ / 18 h / 15 °C

With hydrogen; methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; calcium oxide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1055/s-2007-986664

Reference yield:

: 1000611-99-3
C₁₁H₁₂Br₂N₂O₄

: 1000612-07-6
C₂₇H₃₆N₄O₈SSi

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / ImH / dimethylformamide / 24 h / 20 °C

2: 94 percent / DIBALH / CH₂Cl₂ / 4 h / -78 °C

3: 97 percent / H₂; Et₃N / Pd/C / methanol; CH₂Cl₂ / 5 h / 20 °C

4: 84 percent / MsCl; DBU / 18 h / 0 °C

5: 50 percent / CaO / CH₂Cl₂ / 18 h / 15 °C

With 1H-imidazole; hydrogen; diisobutylaluminium hydride; methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; calcium oxide; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2007-986664