Technology Process of C17H28N4O2S
There total 4 articles about C17H28N4O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
nickel sponge, water wet;
In
tetrahydrofuran;
at 20 ℃;
for 32h;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / acetonitrile / 18 h / 60 °C
2.1: triethylamine / acetonitrile / 0.5 h / 20 °C
2.2: 3 h / 20 °C
3.1: triethylamine / tetrahydrofuran / 15 h / 70 °C
4.1: hydrogen / nickel sponge, water wet / tetrahydrofuran / 32 h / 20 °C / 760.05 Torr
With
hydrogen; caesium carbonate; triethylamine;
nickel sponge, water wet;
In
tetrahydrofuran; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / acetonitrile / 0.5 h / 20 °C
1.2: 3 h / 20 °C
2.1: triethylamine / tetrahydrofuran / 15 h / 70 °C
3.1: hydrogen / nickel sponge, water wet / tetrahydrofuran / 32 h / 20 °C / 760.05 Torr
With
hydrogen; triethylamine;
nickel sponge, water wet;
In
tetrahydrofuran; acetonitrile;