21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

Base Information

Chemical Name:21a2-(phenylmethyl)-2-azaspiro<4.4>nonane
CAS No.:94297-79-7
Molecular Formula:C₁₅H₂₁N
Molecular Weight:215.338
Hs Code.:

Synonyms:21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

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Technology Process of 21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

There total 10 articles about 21a2-(phenylmethyl)-2-azaspiro<4.4>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 136788-14-2
2-(phenylmethyl)-2-azaspiro<4.4>nonan-1-one

: 94297-79-7
21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 0.5h; Ambient temperature;
DOI:10.3987/COM-93-6465

Reference yield:

: 1560-11-8
cyclopent-1-enecarboxylic acid

: 94297-79-7
21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / thionyl chloride

2: 52 percent / triethylamine / benzene / 15.5 h / Heating

3: 26 percent / sodium borohydride / acetonitrile; methanol / 1 h / Irradiation

4: 92 percent / lithium aluminum hydride / diethyl ether / 0.5 h / Ambient temperature

With sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; triethylamine; In methanol; diethyl ether; acetonitrile; benzene;
DOI:10.3987/COM-93-6465

Reference yield:

: 25662-28-6
1-(carboxymethoxy)cyclopentadiene

: 94297-79-7
21a2-(phenylmethyl)-2-azaspiro<4.4>nonane

Guidance literature:: Multi-step reaction with 5 steps

1: 10percent KOH

2: 54 percent / thionyl chloride

3: 52 percent / triethylamine / benzene / 15.5 h / Heating

4: 26 percent / sodium borohydride / acetonitrile; methanol / 1 h / Irradiation

5: 92 percent / lithium aluminum hydride / diethyl ether / 0.5 h / Ambient temperature

With potassium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; triethylamine; In methanol; diethyl ether; acetonitrile; benzene;
DOI:10.3987/COM-93-6465