C₁₄H₁₂ClN

Base Information

• Chemical Name: C₁₄H₁₂ClN
• CAS No.: 1208611-64-6
• Molecular Formula: C₁₄H₁₂ClN
• Molecular Weight: 229.709
• Mol file: 1208611-64-6.mol

Synonyms:C₁₄H₁₂ClN

Chemical Property of C₁₄H₁₂ClN

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₄H₁₂ClN

There total 1 articles about C₁₄H₁₂ClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-chlorophenyl)(p-tolyl)methanone (5953-00-4) → C14H12ClN (1208611-64-6)

Guidance literature:

With 1,1,1,3,3,3-hexamethyl-disilazane; scandium tris(trifluoromethanesulfonate); In toluene; at 90 ℃; for 16h; Temperature; Sealed tube; Inert atmosphere;

DOI:10.1016/j.tet.2020.131864

Reference yield: 88.0%

C14H12ClN (1208611-64-6) + glycine ethyl ester hydrochloride (5680-79-5,883886-67-7) → (E)-methyl 2-(((2-chlorophenyl)(p-tolyl)methylene)amino)acetate

Guidance literature:

In dichloromethane; at 20 - 40 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.6b01273

Reference yield: 85.0%

C14H12ClN (1208611-64-6) + 2-methylphenyl triflate (66107-34-4) → 4-methyl-6-(p-tolyl)phenanthridine (1270093-34-9)

Guidance literature:

With norborn-2-ene; palladium diacetate; caesium carbonate; triphenylphosphine; In acetonitrile; at 90 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ol200174g

upstream raw materials:

(2-chlorophenyl)(p-tolyl)methanone

Downstream raw materials:

4-methyl-6-(p-tolyl)phenanthridine

6-(p-tolyl)benzo[c]phenanthridine