C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

Base Information

Chemical Name:C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O
CAS No.:954145-07-4
Molecular Formula:C₃₁H₄₈O₃Si₂
Molecular Weight:524.891
Hs Code.:

C<sub>16</sub>H<sub>18</sub>SiC<sub>6</sub>H<sub>14</sub>SiC<sub>8</sub>H<sub>12</sub>O<sub>2</sub>CH<sub>2</sub>H<sub>2</sub>O

Synonyms:C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

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Chemical Property of C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

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Technology Process of C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

There total 6 articles about C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 954145-00-7
C₆H₁₄SiC₈H₁₂O₂CH₂H₂O

: 58479-61-1
tert-butylchlorodiphenylsilane

: 954145-07-4
C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1021/ol701783z

Reference yield:

: 954145-06-3
C₆H₁₄SiC₈H₁₂O₃

: 954145-07-4
C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; toluene / 3 h / 90 °C

2.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 766.8 mg / NaOH; H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

3.1: 98 percent / imidazole / dimethylformamide / 3 h / 20 °C

With 1H-imidazole; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1.1: Petasis olefination;
DOI:10.1021/ol701783z

Reference yield:

: 154635-30-0
C₁₀H₁₄O₃O

: 954145-07-4
C₁₆H₁₈SiC₆H₁₄SiC₈H₁₂O₂CH₂H₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: 88 percent / K₂CO₃ / methanol; H₂O / 20 h / 20 °C

2.1: 100 percent / imidazole / dimethylformamide / 36 h / 20 °C

3.1: tetrahydrofuran; toluene / 3 h / 90 °C

4.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 1 h / 0 - 20 °C

4.2: 766.8 mg / NaOH; H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

5.1: 98 percent / imidazole / dimethylformamide / 3 h / 20 °C

With 1H-imidazole; potassium carbonate; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene; 3.1: Petasis olefination;
DOI:10.1021/ol701783z