cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

Base Information

Chemical Name:cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether
CAS No.:263257-26-7
Molecular Formula:C₃₀H₃₉NOSi
Molecular Weight:457.731
Hs Code.:

Synonyms:cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

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Chemical Property of cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

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Technology Process of cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

There total 8 articles about cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4377-41-7
2-Chloromethylquinoline

: 263257-26-7
cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: t-BuOK / tetrahydrofuran / 0.25 h / Heating

3: tetrahydrofuran / 1.5 h / Heating

With potassium tert-butylate; In tetrahydrofuran; toluene; 1: Substitution / 2: dehydrochlorogenation / 3: Wittig reaction;
DOI:10.1021/jm9904102

Reference yield:

: 106166-01-2
(4-bromophenyl)-cyclohexyl methanol

: 263257-26-7
cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / imidazole / dimethylformamide / 14 h / 20 °C

2: 77 percent / n-BuLI / hexane / 1.5 h / -78 - 20 °C

3: tetrahydrofuran / 1.5 h / Heating

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; 1: silylation / 2: Formylation / 3: Wittig reaction;
DOI:10.1021/jm9904102

Reference yield:

: 931-51-1
cyclohexylmagnesiumchloride

: 263257-26-7
cyclohexyl(4-(2-quinol-2-ylethenyl)phenyl)methanol O-tertbutyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / tetrahydrofuran; diethyl ether / 0 - 20 °C

2: 93 percent / imidazole / dimethylformamide / 14 h / 20 °C

3: 77 percent / n-BuLI / hexane / 1.5 h / -78 - 20 °C

4: tetrahydrofuran / 1.5 h / Heating

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; N,N-dimethyl-formamide; 1: Addition / 2: silylation / 3: Formylation / 4: Wittig reaction;
DOI:10.1021/jm9904102