(R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone

Base Information

Chemical Name:(R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone
CAS No.:1234514-02-3
Molecular Formula:C₄₁H₄₆O₆Si
Molecular Weight:662.898
Hs Code.:

Synonyms:(R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone

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Chemical Property of (R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone

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Technology Process of (R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone

There total 1 articles about (R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1234514-03-4
(R,E)-7-(benzyloxy)-6-(tert-butyldiphenylsilyloxy)hept-3-en-2-one

: 81060-27-7
3-cyano-7-methoxyphthalide

: 77-78-1
dimethyl sulfate

: 1234514-02-3
(R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone

Guidance literature:: 3-cyano-7-methoxyphthalide; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.0833333h; Inert atmosphere;

(R,E)-7-(benzyloxy)-6-(tert-butyldiphenylsilyloxy)hept-3-en-2-one; In dimethyl sulfoxide; at 20 ℃; for 0.166667h; Inert atmosphere;

dimethyl sulfate; Further stages;
DOI:10.1016/j.tet.2010.04.048

Reference yield:

: 1234514-02-3
(R)-1-(3-(3-(benzyloxy)-2-(tert-butyldiphenylsilyloxy)propyl)-1,4,8-trimethoxynaphthalen-2-yl)ethanone

: C₂₅H₂₈O₆

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.048