O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

Base Information

Chemical Name:O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate
CAS No.:1311399-46-8
Molecular Formula:C₃₈H₄₁Cl₃N₄O₅Si
Molecular Weight:768.212
Hs Code.:

Synonyms:O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

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Chemical Property of O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

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Technology Process of O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

There total 2 articles about O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1352060-62-8
2-deoxy-2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 1311399-46-8
O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 0.25h;
DOI:10.1021/jo200624e

Reference yield:

: 2-deoxy-2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-α/β-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 1311399-46-8
O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

: O-(2-deoxy-2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl) trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.75h; Overall yield = 94 %; Overall yield = 2 g;
DOI:10.3762/bjoc.14.258

Reference yield: 73.0%

: 1311399-46-8
O-(2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-α-D-galactopyranosyl) trichloroacetimidate

: 1330066-42-6
2-azido-3,4-di-O-benzyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-α-D-galactopyranose

Guidance literature:: With hexamethyldisilathiane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo200624e