methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Base Information

Chemical Name:methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate
CAS No.:130177-74-1
Molecular Formula:C₁₇H₂₀O₆S
Molecular Weight:352.408
Hs Code.:

Synonyms:methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Suppliers and Price of methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

There total 3 articles about methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 130177-70-7
methyl 3α,4α-isopropylidenedioxy-2β-phenylthiocyclohex-5-en-1β-oate

: 130177-74-1
methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 40 ℃; for 72h;
DOI:10.1016/S0040-4020(01)90533-2

Reference yield:

: 88165-26-8,88587-13-7,92936-06-6,99862-07-4,109430-30-0,141393-61-5,141781-67-1
(+/-)-3,4-O,O-isopropylidine-1-methoxycarbonyl-3α,4α,5α-trihydroxycyclohexene

: 130177-74-1
methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / triethylamine / CHCl₃ / 1 h / Ambient temperature

2: 89 percent / m-CPBA / CH₂Cl₂ / 72 h / 40 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;
DOI:10.1016/S0040-4020(01)90533-2

Reference yield:

: 108-98-5
thiophenol

: 130177-74-1
methyl 3α,4α-isopropylidenedioxy-2β-phenylsulphonylcyclohex-5-en-1β-oate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / triethylamine / CHCl₃ / 1 h / Ambient temperature

2: 89 percent / m-CPBA / CH₂Cl₂ / 72 h / 40 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;
DOI:10.1016/S0040-4020(01)90533-2