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Technology Process of [C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]

[C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]

Base Information
  • Chemical Name:[C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]
  • CAS No.:461643-63-0
  • Molecular Formula:C86H80N8O2Zn
  • Molecular Weight:1323.02
  • Hs Code.:
[C<sub>6</sub>H<sub>4</sub>CCC<sub>6</sub>H<sub>4</sub>(Zn(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2)(C<sub>20</sub>H<sub>10</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2))]

Synonyms:[C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]

Suppliers and Price of [C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]
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Chemical Property of [C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]
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Technology Process of [C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]

There total 1 articles about [C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

Zn(II)-5-(3,5-Di-tert-butylphenyl)-10-[4-[2-ethynyl]phenyl]-7,18-dihydro-18,18-dimethyl-17-oxoporphyrin

Zn(II)-5-(3,5-Di-tert-butylphenyl)-10-[4-[2-ethynyl]phenyl]-7,18-dihydro-18,18-dimethyl-17-oxoporphyrin

[(C<sub>20</sub>H<sub>10</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(C<sub>6</sub>H<sub>4</sub>I)(CH<sub>3</sub>)2)]

[(C20H10N4O(C6H3(C(CH3)3)2)(C6H4I)(CH3)2)]

[C<sub>6</sub>H<sub>4</sub>CCC<sub>6</sub>H<sub>4</sub>(Zn(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2)(C<sub>20</sub>H<sub>10</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2))]
461643-63-0

[C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]

Guidance literature:
With tris(dibenzylideneacetone)dipalladium (0); triethylamine; tris-(o-tolyl)phosphine; In toluene; (Ar); weighing of Zn(C20H8N4OMe2(C6H3(t-Bu)2)C6H4CCH), C20H10N4OMe2(C6H3(t-Bu)2)C6H4I), Pd2(dba)3, P(o-tol)3 into Schlenk flask; addn. of C7H8/Et3N (5:1); stirring at 35°C for 3.5 h; addn. of Pd2(dba)3, P(o-tol)3(Chem. Mater. 1999, 11, 2974-2983); after 4.5 h removal of solvent, chromy. (silica, CH2Cl2), concn. to dryness, dissolving in THF, chromy. in four equial portions (SEC, THF) with gravity elution, combining of fractions, chromy. (silica, CH2Cl2), elem.anal.;
DOI:10.1021/ja035987u

Reference yield: 34.0%

[C<sub>6</sub>H<sub>4</sub>CCC<sub>6</sub>H<sub>4</sub>(Zn(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2)(C<sub>20</sub>H<sub>10</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2))]
461643-63-0

[C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2)(C20H10N4O(C6H3(C(CH3)3)2)(CH3)2))]

zinc(II) acetate dihydrate
5970-45-6

zinc(II) acetate dihydrate

[C<sub>6</sub>H<sub>4</sub>CCC<sub>6</sub>H<sub>4</sub>(Zn(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>O(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)(CH<sub>3</sub>)2))2]

[C6H4CCC6H4(Zn(C20H8N4O(C6H3(C(CH3)3)2)(CH3)2))2]

Guidance literature:
In methanol; dichloromethane; (Ar); treatment of soln. of (Zn(C20H8N4OMe2(C6H3(t-Bu)2)C6H4CCH))(C20H10N4OMe2(C6H3(t-Bu)2))(C6H4CCC6H4) in CH2Cl2/methanol (1:1) with Zn(OAc)2*2H2O; stirring for 14 h; removal of solvent, chromy. (silica, CH2Cl2/hexanes (1:1), ethyl acetate), elem. anal.;
DOI:10.1021/ja035987u
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