C₂₉H₄₆O₈SSi

Base Information

Chemical Name:C₂₉H₄₆O₈SSi
CAS No.:1316846-41-9
Molecular Formula:C₂₉H₄₆O₈SSi
Molecular Weight:582.831
Hs Code.:

C<sub>29</sub>H<sub>46</sub>O<sub>8</sub>SSi

Synonyms:C₂₉H₄₆O₈SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₆O₈SSi

Chemical Property:

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Technology Process of C₂₉H₄₆O₈SSi

There total 8 articles about C₂₉H₄₆O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1316846-40-8
C₂₅H₃₈O₆SSi

: 107-30-2
chloromethyl methyl ether

: 1316846-41-9
C₂₉H₄₆O₈SSi

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 6h;

Reference yield:

: C₁₄H₁₈O₄

: 1316846-41-9
C₂₉H₄₆O₈SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -40 °C

1.2: 1 h / 0 °C

2.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C

2.2: 2.17 h / -78 °C

2.3: -78 - 20 °C

3.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C

4.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C

5.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

6.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C

6.2: 1 h / 0 - 20 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C

With 1H-imidazole; dmap; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; acetonitrile;

Reference yield:

: C₁₉H₂₀O₄S

: 1316846-41-9
C₂₉H₄₆O₈SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C

1.2: 2.17 h / -78 °C

1.3: -78 - 20 °C

2.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C

3.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C

4.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

5.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C

5.2: 1 h / 0 - 20 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C

With 1H-imidazole; dmap; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile;