1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

Base Information

Chemical Name:1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide
CAS No.:104330-97-4
Molecular Formula:BrH*C₂₀H₂₄N₂O₂
Molecular Weight:405.335
Hs Code.:

Synonyms:1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

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Chemical Property of 1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

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Technology Process of 1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

There total 2 articles about 1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 93598-53-9
N^α-cyclohexylthiocarbonyl-1-methyltryptophan methyl ester

: 104330-97-4
1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

Guidance literature:: With 1-bromomethyl-4-nitro-benzene; In acetonitrile; for 4h; Heating;
DOI:10.1248/cpb.33.3237

Reference yield:

: 104331-11-5
2-(Cyclohexanecarbonyl-amino)-3-(1-methyl-1H-indol-3-yl)-propionic acid methyl ester

: 104330-97-4
1-cyclohexyl-3-methoxycarbonyl-9-methyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Lawesson's reagent / 1,2-dimethoxy-ethane / 3 h / Ambient temperature

2: 76 percent / 4-nitrobenzyl bromide / acetonitrile / 4 h / Heating

With Lawessons reagent; 1-bromomethyl-4-nitro-benzene; In 1,2-dimethoxyethane; acetonitrile;
DOI:10.1248/cpb.33.3237