Technology Process of C17H18N2O3
There total 5 articles about C17H18N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
acetonitrile;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1016/j.tetlet.2011.10.026
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
3: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0 - 20 °C / Inert atmosphere
With
thionyl chloride; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.10.026
- Guidance literature:
-
Multi-step reaction with 3 steps
1: samarium diiodide; isopropyl alcohol / tetrahydrofuran / Inert atmosphere
2: triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
3: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0 - 20 °C / Inert atmosphere
With
samarium diiodide; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; isopropyl alcohol;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.10.026