5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

Base Information

Chemical Name:5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide
CAS No.:716379-27-0
Molecular Formula:C₁₂H₁₂N₆O
Molecular Weight:256.267
Hs Code.:

5-amino-1-benzyl-3-methyl-1<i>H</i>-pyrazole-4-carbonyl azide

Synonyms:5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

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Chemical Property of 5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

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Technology Process of 5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

There total 1 articles about 5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 716379-23-6
5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carboxylic acid hydrazide

: 716379-27-0
5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

Guidance literature:: With acetic acid; sodium nitrite; In water; at 0 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2004.03.142

Reference yield: 35.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 716379-27-0
5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

: 716379-30-5
(5-amino-1-benzyl-3-methyl-1H-pyrazol-4-yl)-carbamic acid benzyl ester

Guidance literature:: In xylene; Heating;
DOI:10.1016/j.tetlet.2004.03.142

Reference yield:

: 716379-27-0
5-amino-1-benzyl-3-methyl-1H-pyrazole-4-carbonyl azide

: 1-benzyl-3-methyl-1H-pyrazolo[3,4-b]pyrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / xylene / Heating

2: H₂ / Pd/C / methanol / 1.5 h / 20 °C

3: ethanol / 20 °C

With hydrogen; palladium on activated charcoal; In methanol; ethanol; xylene;
DOI:10.1016/j.tetlet.2004.03.142