C₅₀H₆₄O₈Si

Base Information

Chemical Name:C₅₀H₆₄O₈Si
CAS No.:1352816-07-9
Molecular Formula:C₅₀H₆₄O₈Si
Molecular Weight:821.139
Hs Code.:

C<sub>50</sub>H<sub>64</sub>O<sub>8</sub>Si

Synonyms:C₅₀H₆₄O₈Si

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Chemical Property of C₅₀H₆₄O₈Si

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Technology Process of C₅₀H₆₄O₈Si

There total 1 articles about C₅₀H₆₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: C₄₇H₆₀O₈Si

: 106-95-6
allyl bromide

: 1352816-07-9
C₅₀H₆₄O₈Si

Guidance literature:: C₄₇H₆₀O₈Si; With potassium hexamethylsilazane; In tetrahydrofuran; at -20 ℃; for 1h;

With 18-crown-6 ether; In tetrahydrofuran; at -20 ℃; for 0.0833333h;

allyl bromide; In tetrahydrofuran; at -20 - -5 ℃; for 0.833333h;
DOI:10.1002/anie.201104681

Reference yield: 40.0%

: 1352816-07-9
C₅₀H₆₄O₈Si

: 1352816-08-0
C₅₀H₆₄O₈Si

Guidance literature:: In o-xylene; at 165 ℃; for 20h; Inert atmosphere;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-07-9
C₅₀H₆₄O₈Si

: 1352816-12-6
C₃₃H₄₄O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: o-xylene / 20 h / 165 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

2.2: NaBO₃*4H₂O / 3 h / 20 °C

3.1: pyridine; dmap / dichloromethane / 1 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

5.1: pyridine; tributylphosphine / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide / dichloromethane; water / 29 h / 20 °C / pH 7 / aq. phosphate buffer

7.1: cerium(III) chloride heptahydrate; oxalic acid / acetonitrile / 2 h / 20 °C

With pyridine; dmap; tributylphosphine; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; oxalic acid; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; o-xylene; water; acetonitrile; 2.1: Hydroboration reaction;
DOI:10.1002/anie.201104681