Technology Process of C33H32N2O9
There total 10 articles about C33H32N2O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triflic azide;
In
hexane; acetonitrile;
at -30 - 24 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja307497h
- Guidance literature:
-
With
triflic azide;
In
hexane; dichloromethane;
at -20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja200034b
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: methanesulfonamide / tetrahydrofuran; tert-butyl alcohol / Inert atmosphere
2.1: oxygen; palladium diacetate / dimethyl sulfoxide / Inert atmosphere
3.1: pyridinium p-toluenesulfonate / toluene / 12 h / 10 - 24 °C / Inert atmosphere
4.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.5 h / -50 - 24 °C / Inert atmosphere
4.2: 1.5 h / -78 - 24 °C / Inert atmosphere
4.3: 12 h / 24 °C / Inert atmosphere
5.1: tris(diethylamino)sulfonium difluorotrimethylsiliconate / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
6.1: palladium diacetate; triphenylphosphine; silver carbonate / toluene / 2 h / 80 °C / Inert atmosphere
7.1: dmap; triflic azide / hexane; acetonitrile / 2 h / -30 - 24 °C / Inert atmosphere
With
dmap; copper(l) iodide; methanesulfonamide; triflic azide; tris(diethylamino)sulfonium difluorotrimethylsiliconate; oxygen; palladium diacetate; pyridinium p-toluenesulfonate; triphenylphosphine; silver carbonate;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja307497h
