(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

Base Information

Chemical Name:(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone
CAS No.:391913-59-0
Molecular Formula:C₃₅H₂₇N₃O₃
Molecular Weight:537.618
Hs Code.:

(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[<i>c</i>]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

Synonyms:(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

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Chemical Property of (1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

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Technology Process of (1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

There total 5 articles about (1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 391913-58-9
(6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

: 391913-59-0
(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; ethanol; for 4h; Heating;
DOI:10.1016/S0040-4039(01)01915-3

Reference yield:

: 391913-74-9
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carboxylic acid

: 391913-59-0
(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / carbonyl-diimidazole / dimethylformamide / 2 h / -10 °C

2: 60 percent / CuTc; trifurylphosphine / Pd₂dba3*CHCl₃ / tetrahydrofuran / 18 h / 50 °C

3: 63 percent / aq. KOH / tetrahydrofuran; ethanol / 4 h / Heating

With potassium hydroxide; Carbonyldiimidazole; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)01915-3

Reference yield:

: 391913-53-4
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carboxylic acid ethyl ester

: 391913-59-0
(1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluoren-4-yl)-(4-benzyloxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / LiOH / tetrahydrofuran; H₂O; methanol / 5 h / 20 °C

2: 58 percent / carbonyl-diimidazole / dimethylformamide / 2 h / -10 °C

3: 60 percent / CuTc; trifurylphosphine / Pd₂dba3*CHCl₃ / tetrahydrofuran / 18 h / 50 °C

4: 63 percent / aq. KOH / tetrahydrofuran; ethanol / 4 h / Heating

With potassium hydroxide; lithium hydroxide; Carbonyldiimidazole; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)01915-3