(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

Base Information

Chemical Name:(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal
CAS No.:935534-00-2
Molecular Formula:C₁₈H₂₈O₄
Molecular Weight:308.418
Hs Code.:

Synonyms:(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

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Chemical Property of (S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

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Technology Process of (S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

There total 14 articles about (S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1381862-11-8
(R)-1-(3-methoxypropoxy)-2-methoxy-5-(2-isopropyl-4-pentenyl)benzene

: 935534-00-2
(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 0 ℃; for 4h;
DOI:10.1039/c4ob01963f

Reference yield:

: 37942-01-1
5-bromo-2-methoxyphenol

: 935534-00-2
(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; potassium iodide / acetonitrile / 24 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C

2.2: 1 h / -78 - 20 °C

3.1: aluminum (III) chloride; lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C

4.1: osmium(VIII) oxide; sodium periodate; 1,4-diaza-bicyclo[2.2.2]octane / tetrahydrofuran; water; tert-butyl alcohol / 4 h / 0 °C

With 1,4-diaza-bicyclo[2.2.2]octane; aluminum (III) chloride; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; potassium carbonate; potassium iodide; In tetrahydrofuran; diethyl ether; hexane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1039/c4ob01963f

Reference yield:

: 960124-88-3
(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanenitrile

: 935534-00-2
(S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanal

Guidance literature:: (S)-3-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-4-methyl-pentanenitrile; With diisobutylaluminium hydride; In ethyl acetate; toluene; at -65 - 20 ℃;

With ammonium chloride; In water; ethyl acetate; toluene; at 0 ℃; for 1h;

With sulfuric acid; In diethyl ether; water; ethyl acetate; toluene; at 20 ℃; for 1h;