(S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

Base Information

Chemical Name:(S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]
CAS No.:1198620-69-7
Molecular Formula:C₁₆H₁₇N₃O₅
Molecular Weight:331.328
Hs Code.:

Synonyms:(S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

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Chemical Property of (S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

Chemical Property:

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Technology Process of (S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

There total 5 articles about (S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1198621-36-1
C₃₀H₂₉N₃O₅

: 1198620-69-7
(S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; for 1h;

Reference yield:

: 62489-21-8
9-benzyloxy-3,3-dimethyl-1,5-dihydro-[1,3]dioxepino[5,6-c]pyridine-8-carboxylic acid methyl ester

: 1198620-69-7
(S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

1.2: 0.5 h / -78 °C

2.1: formic acid / tetrahydrofuran; water / 2 h / 70 °C

3.1: manganese(IV) oxide / dichloromethane / 20 °C

4.1: 0.33 h / 70 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h

With manganese(IV) oxide; formic acid; hydrogen; lithium hexamethyldisilazane; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 1198621-04-3
N,3-bis(benzyloxy)-4,5-bis(hydroxymethyl)picolinamide

: 1198620-69-7
(S)-(-)-3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 2-hydroxyamide 5-[(1-phenyl-ethyl)-amide]

Guidance literature:: Multi-step reaction with 3 steps

1: manganese(IV) oxide / dichloromethane / 20 °C

2: 0.33 h / 70 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 1 h

With manganese(IV) oxide; hydrogen; palladium 10% on activated carbon; In methanol; dichloromethane;