(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Base Information

Chemical Name:(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid
CAS No.:1412697-21-2
Molecular Formula:C₂₁H₂₈N₄O₇
Molecular Weight:448.476
Hs Code.:

Synonyms:(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Suppliers and Price of (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

There total 3 articles about (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1412697-17-6
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine methyl ester

: 1412697-21-2
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Guidance literature:: With water; barium(II) hydroxide; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1002/ejoc.201200463

Reference yield:

: 668990-26-9
6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonic acid

: 1412697-21-2
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

1.2: 20 h / 20 °C / Inert atmosphere

2.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

With O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate; water; barium(II) hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201200463

Reference yield:

: 229643-36-1
methyl 6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonate

: 1412697-21-2
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

2.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

2.2: 20 h / 20 °C / Inert atmosphere

3.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

With O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate; water; barium(II) hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201200463