tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane
CAS No.:1463523-02-5
Molecular Formula:C₃₁H₃₆O₄Si
Molecular Weight:500.71
Hs Code.:

Synonyms:tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

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Chemical Property of tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

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Technology Process of tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

There total 3 articles about tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1463522-99-7
C₂₈H₃₄O₄Si

: 106-96-7
propargyl bromide

: 1463523-02-5
tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

Guidance literature:: With potassium carbonate; In ⁽²⁾H₈-toluene; acetone;
DOI:10.1039/c3cc44799e

Reference yield:

: 2150-46-1
Methyl 2,5-dihydroxybenzoate

: 1463523-02-5
tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; dibutyl ether / 144 h / 20 °C

2: para-xylene / 16 h / 140 °C

3: potassium carbonate / acetone; ⁽²⁾H₈-toluene

With potassium carbonate; In tetrahydrofuran; dibutyl ether; para-xylene; ⁽²⁾H₈-toluene; acetone;
DOI:10.1039/c3cc44799e

Reference yield:

: 490-79-9
2,5-dihydroxybenzoic acid.

: 1463523-02-5
tert-butyl(2-(4,4-diphenyl-6-(prop-2-yn-1-yloxy)-4H-benzo-[d][1,3]dioxin-2-yl)ethoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 45 h / Reflux

2: tetrahydrofuran; dibutyl ether / 144 h / 20 °C

3: para-xylene / 16 h / 140 °C

4: potassium carbonate / acetone; ⁽²⁾H₈-toluene

With sulfuric acid; potassium carbonate; In tetrahydrofuran; dibutyl ether; para-xylene; ⁽²⁾H₈-toluene; acetone;
DOI:10.1039/c3cc44799e