16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile

Base Information

Chemical Name:16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile
CAS No.:1263292-63-2
Molecular Formula:C₈₇H₉₇NO₇
Molecular Weight:1268.73
Hs Code.:

Synonyms:16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile

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Chemical Property of 16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile

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Technology Process of 16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile

There total 1 articles about 16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1263292-52-9,1263292-51-8
8,9-bis(heptyloxy)-16-hydroxytetraphenylene-1-carbonitrile

: 1263292-57-4
1-(benzyloxy)-16-(3-bromopropoxy)-8,9-bis(heptyloxy)tetraphenylene

: 1263292-63-2
16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1016/j.tet.2010.10.064

Reference yield:

: 1263292-63-2
16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile

: 1263292-87-0
C₈₇H₉₈O₈

Guidance literature:: 16-(3-(16-(benzyloxy)-8,9-bis(heptyloxy)tetraphenylen-1-yloxy)prop-oxy)-8,9-bis(heptyloxy)tetraphenylene-1-carbonitrile; With diisobutylaluminium hydride; In dichloromethane; cyclohexane; at -78 ℃; for 1h;

With hydrogenchloride; water; In dichloromethane; cyclohexane; at -78 - 20 ℃;
DOI:10.1016/j.tet.2010.10.064