Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester

Base Information

• Chemical Name: Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester
• CAS No.: 185805-21-4
• Molecular Formula: C₃₀H₃₀N₂O₆Si
• Molecular Weight: 542.663

Synonyms:Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester

Chemical Property of Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester

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Technology Process of Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester

There total 1 articles about Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenylsilyl dichloride (80-10-4) + 3-((R)-2-Hydroxy-1-phenyl-ethyl)-6-methyl-3,6-diaza-bicyclo[3.1.0]hexane-2,4-dione + 2-hydroxyethyl acrylate (818-61-1,9051-31-4,26022-14-0) → Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester (185805-21-4)

Guidance literature:

With triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C - 3 h, room temperature - overnight, 2.) CH₂Cl₂, 1 h;

DOI:10.1021/jo9609034

Reference yield: 46.0%

Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester (185805-21-4) → C30H30N2O6Si + C30H30N2O6Si

Guidance literature:

With isoprene; In acetonitrile; Yield given; Irradiation;

DOI:10.1021/jo00101a005

Reference yield: 46.0%

Acrylic acid 2-{[(R)-2-(6-methyl-2,4-dioxo-3,6-diaza-bicyclo[3.1.0]hex-3-yl)-2-phenyl-ethoxy]-diphenyl-silanyloxy}-ethyl ester (185805-21-4) → C30H30N2O6Si + C30H30N2O6Si (185805-22-5)

Guidance literature:

With isoprene; In acetonitrile; Title compound not separated from byproducts; Irradiation;

DOI:10.1021/jo9609034

upstream raw materials:

diphenylsilyl dichloride

2-hydroxyethyl acrylate

Downstream raw materials:

C₃₀H₃₀N₂O₆Si

(1R,5S,6R)-3-((R)-2-Hydroxy-1-phenyl-ethyl)-8-methyl-2,4-dioxo-3,8-diaza-bicyclo[3.2.1]octane-6-carboxylic acid methyl ester

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