2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol

Base Information

• Chemical Name: 2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol
• CAS No.: 728028-60-2
• Molecular Formula: C₂₈H₂₄O₂
• Molecular Weight: 392.497
• Mol file: 728028-60-2.mol

Synonyms:2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol

Chemical Property of 2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol

There total 1 articles about 2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethylanthraquinone (6531-35-7) + phenylmagnesium bromide → 2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol (728028-60-2)

Guidance literature:

With dibutyl ether; at 100 ℃; optically inactive isomer of mp: 229 degree Celsius;

DOI:10.1021/ja01866a042

Reference yield:

2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol (728028-60-2) → 2,3-dimethyl-9,10-diphenylanthracene (61415-64-3)

Guidance literature:

With hydrogen iodide;

Reference yield:

2,3-dimethyl-9,10-diphenyl-9,10-dihydro-anthracene-9,10-diol (728028-60-2) → 2,3-dimethyl-9,10-diphenyl-9,10-dihydro-9,10-epidioxido-anthracene

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous HI

2: CS₂; air / Irradiation_.mit Sonnenlicht

With carbon disulfide; air; hydrogen iodide;

upstream raw materials:

2,3-dimethylanthraquinone

Downstream raw materials:

2,3-dimethyl-9,10-diphenylanthracene