Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate

Base Information

Chemical Name:Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate
CAS No.:725746-36-1
Molecular Formula:C₁₂H₁₁NO₃
Molecular Weight:217.224
Hs Code.:
DSSTox Substance ID:DTXSID201229962
Nikkaji Number:J2.071.875G

Synonyms:DTXSID201229962;725746-36-1;Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate

Suppliers and Price of Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:217.07389321
Heavy Atom Count:16
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CN(C(=O)C=C1)C(=O)OC2=CC=CC=C2

Technology Process of Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate

There total 2 articles about Phenyl 5,6-dihydro-2-oxo-1(2H)-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-oxo-3-phenylselanyl-piperidine-1-carboxylic acid phenyl ester

: 725746-36-1
N-phenoxycarbonyl-5,6-dihydro-2(1H)-pyridone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1039/b403793f

Reference yield:

: 164732-57-4
N-(phenyloxycarbonyl)piperidin-2-one

: 725746-36-1
N-phenoxycarbonyl-5,6-dihydro-2(1H)-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: LHMDS

2: MCPBA

With 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane;
DOI:10.1039/b403793f

Reference yield:

: 557-20-0
diethylzinc

: 106-95-6
allyl bromide

: 725746-36-1
N-phenoxycarbonyl-5,6-dihydro-2(1H)-pyridone

: (3S,4S)-N-phenoxycarbonyl-3-(2-propenil)-4-ethyl-2-piperidinone

: (3R,4R)-N-phenoxycarbonyl-3-(2-propenil)-4-ethyl-2-piperidinone

: cis-N-phenoxycarbonyl-3-(2-propenil)-4-ethyl-2-piperidinone

Guidance literature:: diethylzinc; N-phenoxycarbonyl-5,6-dihydro-2(1H)-pyridone; With [(R)-1,1'-binaphthyl-2,2'-diyldioxy]{bis[(S)-(1-phenylethyl)]amino}phosphine; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; toluene; at -78 ℃; for 2h;

allyl bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene; at 0 ℃; for 16h; Title compound not separated from byproducts;
DOI:10.1039/b403793f