hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇

Base Information

Chemical Name:hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇
CAS No.:74125-54-5
Molecular Formula:C₂₅H₃₂B₇PRu
Molecular Weight:540.25
Hs Code.:

hyper-closo-2,3-(CH<sub>3</sub>)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC<sub>2</sub>B<sub>7</sub>H<sub>7</sub>

Synonyms:hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇

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Chemical Property of hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇

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Technology Process of hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇

There total 1 articles about hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76601-83-7
hyper-closo-2,3-(CH₃)2-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

: 13271-06-2
o-diphenylphosphinoallylbenzene

: 74125-54-5
hyper-closo-2,3-(CH₃)2-6-(o-allylphenyl)diphenylphosphine-6,2,3-RuC₂B₇H₇

Guidance literature:: In toluene; byproducts: P(C6H5)3; (N2 or Ar); a soln. of Ru-complex and P-compound stirred overnight at room temp.; layered with pentane; cooled to -15°C for 3 days; filtered of inair; washed with methanol and pentane; dried in vacuo; elem. anal.;
DOI:10.1021/ja00538a014