E-3-benzyloxy-2-propenyl glycolate

Base Information

Chemical Name:E-3-benzyloxy-2-propenyl glycolate
CAS No.:853888-63-8
Molecular Formula:C₁₇H₂₂O₄
Molecular Weight:290.359
Hs Code.:

Synonyms:E-3-benzyloxy-2-propenyl glycolate

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Chemical Property of E-3-benzyloxy-2-propenyl glycolate

Chemical Property:

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Technology Process of E-3-benzyloxy-2-propenyl glycolate

There total 3 articles about E-3-benzyloxy-2-propenyl glycolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 160239-22-5
2-(pent-4-en-1-yloxy)acetic acid

: 853888-62-7
(E)-3-benzyloxyprop-2-en-1-ol

: 853888-63-8
E-3-benzyloxy-2-propenyl glycolate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 23 ℃;
DOI:10.1016/j.tetlet.2005.03.114

Reference yield:

: 127762-21-4
methyl (E)-β-benzyloxyacrylate

: 853888-63-8
E-3-benzyloxy-2-propenyl glycolate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / DIBAH / CH₂Cl₂ / 1 h / -78 °C

2: 93 percent / DCC; DMAP / CH₂Cl₂ / 0 - 23 °C

With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2005.03.114

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 853888-63-8
E-3-benzyloxy-2-propenyl glycolate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Me₃P / CH₂Cl₂ / 0.5 h / 0 °C

2: 93 percent / DIBAH / CH₂Cl₂ / 1 h / -78 °C

3: 93 percent / DCC; DMAP / CH₂Cl₂ / 0 - 23 °C

With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; trimethylphosphane; In dichloromethane;
DOI:10.1016/j.tetlet.2005.03.114