1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol

Base Information

• Chemical Name: 1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol
• CAS No.: 1391099-72-1
• Molecular Formula: C₁₀₀H₁₂₀O₁₇
• Molecular Weight: 1594.04

Synonyms:1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol

Chemical Property of 1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol

Chemical Property:

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Technology Process of 1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol

There total 2 articles about 1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1-O-allyl-4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol (1391099-71-0) → 1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol (1391099-72-1)

Guidance literature:

With 5-methyl-1,3-benzodioxole; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jo301189y

Reference yield: 58.0%

1-O-allyl-4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol (1391099-71-0) → 1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol (1391099-72-1) + 1-O-allyl-4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxy-(6-(4-(3,4-imethoxyphenyl)benzyl))phenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-palmitoyl-α-D-mannopyranosyl)-D-myo-inositol (1434820-81-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jo4004184

Reference yield: 84.0%

1-O-allyl-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol (1391099-72-1) + stearic acid (57-11-4) → 1-O-allyl-4,5-di-O-benzyl-3-O-octadecanoyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol (1391099-73-2)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

DOI:10.1021/jo301189y

upstream raw materials:

1-O-allyl-4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol

Downstream raw materials:

1-O-allyl-4,5-di-O-benzyl-3-O-octadecanoyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-2-O-(2,3,4-tri-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-D-myo-inositol

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