6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

Base Information

Chemical Name:6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene
CAS No.:545358-10-9
Molecular Formula:C₃₃H₃₂N₂O₄
Molecular Weight:520.628
Hs Code.:

Synonyms:6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

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Chemical Property of 6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

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Technology Process of 6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

There total 3 articles about 6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 5,7-dihydro-dibenzo[a,c]cycloheptene-6,6-dicarbonyl dichloride

: 545358-10-9
6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/S0040-4020(03)00144-3

Reference yield:

: 6672-66-8
5,7-dihydro-dibenzo[a,c]cycloheptene-6,6-dicarboxylic acid diethyl ester

: 545358-10-9
6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / methanol / 8 h / Heating

2: SOCl₂ / 2 h / Heating

3: 1.08 g / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With sodium hydroxide; thionyl chloride; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(03)00144-3

Reference yield:

: 109339-05-1
dibenzo[a,c]-1,3-cycloheptadiene-6,6-dicarboxylic acid

: 545358-10-9
6,6-bis[N-(1'S)-(1'-phenyl-2'-hydroxyethyl)carbamoyl]dibenzo[a,c]-1,3-cycloheptadiene

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 2 h / Heating

2: 1.08 g / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(03)00144-3