2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

Base Information

Chemical Name:2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)
CAS No.:303186-03-0
Molecular Formula:C₅₃H₆₃NO₁₆SSi
Molecular Weight:1030.23
Hs Code.:

Synonyms:2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

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Technology Process of 2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

There total 1 articles about 2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 165065-08-7
2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel

: 303186-02-9
2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (β)

: 303186-03-0
2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

Guidance literature:: With dmap; thionyl chloride; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1016/S0040-4020(00)00611-6

Reference yield: 98.0%

: 303186-03-0
2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

: 6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

Guidance literature:: With pyridine hydrogenfluoride; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1016/S0040-4020(00)00611-6

Reference yield: 98.0%

: 303186-03-0
2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfite (α)

: 303186-05-2
2'-O-(tert-butyldimethylsilyl)-6α-hydroxy-7-epipaclitaxel 6,7-O,O'-cyclosulfate

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 1.5h;
DOI:10.1016/S0040-4020(00)00611-6