C₃₁H₃₄N₂O₆

Base Information

Chemical Name:C₃₁H₃₄N₂O₆
CAS No.:1613707-80-4
Molecular Formula:C₃₁H₃₄N₂O₆
Molecular Weight:530.621
Hs Code.:

C<sub>31</sub>H<sub>34</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₁H₃₄N₂O₆

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Chemical Property of C₃₁H₃₄N₂O₆

Chemical Property:

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Technology Process of C₃₁H₃₄N₂O₆

There total 12 articles about C₃₁H₃₄N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1613707-79-1
C₂₀H₂₂F₃NO₇S

: 149965-78-6
N-benzyloxycarbonyl-but-3-ynyl-1-amine

: 1613707-80-4
C₃₁H₃₄N₂O₆

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; triethylamine; In hexane; acetonitrile; for 18h; Inert atmosphere; Reflux;

Reference yield:

: 3453-33-6
6-methoxynaphthalene-2-carbaldehyde

: 1613707-80-4
C₃₁H₃₄N₂O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C

1.2: 16 h / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethyl acetate / 16 h / 20 °C / 760.05 Torr

3.1: water; sodium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C

4.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 0.02 h / -78 °C

4.2: 1.17 h / -78 - 20 °C

5.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

5.2: 0.08 h / -78 °C

5.3: 16 h / -78 - 24 °C

6.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.17 h / 0 - 20 °C

7.1: palladium 10% on activated carbon; hydrogen / water / 3 h / 20 °C / 760.05 Torr

8.1: acetic acid; hydrogen bromide / 3 h / Reflux

9.1: acetyl chloride / 4 h / 0 °C / Reflux

10.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

11.1: pyridine / dichloromethane / 3 h / 0 - 20 °C

12.1: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 18 h / Inert atmosphere; Reflux

With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

: 744241-46-1
methyl (E)-3-(6-methoxynaphthalen-2-yl)acrylate

: 1613707-80-4
C₃₁H₃₄N₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethyl acetate / 16 h / 20 °C / 760.05 Torr

2.1: water; sodium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C

3.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 0.02 h / -78 °C

3.2: 1.17 h / -78 - 20 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: 0.08 h / -78 °C

4.3: 16 h / -78 - 24 °C

5.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.17 h / 0 - 20 °C

6.1: palladium 10% on activated carbon; hydrogen / water / 3 h / 20 °C / 760.05 Torr

7.1: acetic acid; hydrogen bromide / 3 h / Reflux

8.1: acetyl chloride / 4 h / 0 °C / Reflux

9.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

10.1: pyridine / dichloromethane / 3 h / 0 - 20 °C

11.1: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 18 h / Inert atmosphere; Reflux

With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; acetonitrile;