N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

Base Information

Chemical Name:N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide
CAS No.:1431153-06-8
Molecular Formula:C₁₆H₂₁F₃N₂O₃
Molecular Weight:346.35
Hs Code.:

Synonyms:N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

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Chemical Property of N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

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Technology Process of N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

There total 3 articles about N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1037093-50-7
N-(tert-butoxycarbonyl)-3-vinylaniline

: Umemoto's reagent

: 75-05-8,26809-02-9
acetonitrile

: 1431153-06-8
N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

Guidance literature:: With 2,6-dimethylpyridine; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; water; at 20 ℃; for 3h; regioselective reaction; Inert atmosphere; UV-irradiation; Schlenk technique;
DOI:10.1021/ol4006272

Reference yield: 75.0%

: 1431153-06-8
N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

Guidance literature:: With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; water; at 20 ℃; for 3h; Schlenk technique; Irradiation;

Reference yield:

: 25216-74-4
tert-butyl (3-bromophenyl)carbamate

: 1431153-06-8
N-{1-[(3-tert-butoxycarbonylamino)phenyl]-3,3,3-trifluoropropyl}acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium dichloride; triphenylphosphine; caesium carbonate / tetrahydrofuran; water / 22 h / 80 °C / Inert atmosphere; Schlenk technique

2: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; water; 2,6-dimethylpyridine / 3 h / 20 °C / Inert atmosphere; UV-irradiation; Schlenk technique

With 2,6-dimethylpyridine; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; water; caesium carbonate; triphenylphosphine; palladium dichloride; In tetrahydrofuran; water;
DOI:10.1021/ol4006272