bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

Base Information

Chemical Name:bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate
CAS No.:163778-63-0
Molecular Formula:C₇₂H₁₀₄N₁₀O₁₈
Molecular Weight:1397.67
Hs Code.:

bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

Synonyms:bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

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Chemical Property of bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

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Technology Process of bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

There total 2 articles about bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 17134-17-7
triethylene glycol bis(chloroformate)

: 163778-62-9
bis(phenylmethyl) 8,16-dioxo-2,9,12,15,22-pentaazatricosanedioate

: 163778-63-0
bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 40 ℃; for 1h;
DOI:10.1021/jm00012a013

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 163778-63-0
bis(phenylmethyl) 8,13,24,29-tetraoxo-12,25-bis<2-<<1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>ethyl>-14,17,20,23-tetraoxa-2,9,12,25,28,35-hexaazahexatriacontanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) carbonyldiimidazole, 2.) Et₃N / 1.) EtOAc, RT, 1.5 h, 2.) EtOAc, 4 h

2: 60 percent / pyridine / dimethylformamide / 1 h / 40 °C

With pyridine; triethylamine; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide;
DOI:10.1021/jm00012a013