11,12-dideuterio-13-cis-retinal

Base Information

Chemical Name:11,12-dideuterio-13-cis-retinal
CAS No.:74430-64-1
Molecular Formula:C₂₀H₂₈O
Molecular Weight:286.426
Hs Code.:

Synonyms:11,12-dideuterio-13-cis-retinal

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Chemical Property of 11,12-dideuterio-13-cis-retinal

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Technology Process of 11,12-dideuterio-13-cis-retinal

There total 14 articles about 11,12-dideuterio-13-cis-retinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103633-89-2
3-(β-ionilidene)-1-propyne

: 74352-09-3,74410-13-2,74410-14-3,74430-64-1
C₂₀H₂₆⁽²⁾H₂O

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / BuLi / tetrahydrofuran; hexane / 1 h / -60 deg C to room t.

2: 1.) LiAlD₄ 2.) D₂O / 1.) ether, 3 h, reflux, 2.) ether

With n-butyllithium; lithium aluminium deuteride; water-d2; In tetrahydrofuran; hexane;

Reference yield:

: 103633-89-2
3-(β-ionilidene)-1-propyne

: 74430-64-1
11,12-dideuterio-13-cis-retinal

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / BuLi / tetrahydrofuran; hexane / 1 h / -60 deg C to room t.

2: 1.) LiAlD₄ 2.) D₂O / 1.) ether, 3 h, reflux, 2.) ether

With n-butyllithium; lithium aluminium deuteride; water-d2; In tetrahydrofuran; hexane;

Reference yield:

: 79-77-6,14901-07-6
(E)-β-ionone

: 74430-64-1
11,12-dideuterio-13-cis-retinal

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Mg, 2.) HgCl₂ / 1.) Et₂O

2: 90 percent / 4-dimethylaminopyridine / toluene

3: 92 percent / 1,5-diazabicyclo<4.3.0>non-5-ene, NaNH₂ / toluene / Heating

4: 90 percent / BuLi / tetrahydrofuran / -60 °C

5: 1.) LiAlD₄, 2.) D₂O / 1.) Et₂O

With dmap; n-butyllithium; lithium aluminium deuteride; DBN; water-d2; sodium amide; magnesium; mercury dichloride; In tetrahydrofuran; toluene;
DOI:10.1021/ja00536a046