1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

Base Information

Chemical Name:1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose
CAS No.:869384-37-2
Molecular Formula:C₄₀H₃₂O₁₀S
Molecular Weight:704.754
Hs Code.:

Synonyms:1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

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Chemical Property of 1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

Chemical Property:

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Technology Process of 1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

There total 3 articles about 1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13992-16-0,23661-28-1,24404-53-3,28512-68-7,65236-85-3,86782-39-0,108032-93-5,121524-01-4,121570-34-1
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(phenylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 869384-37-2
1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate; methanol

2: pyridine; dmap / 0 °C

3: urea hydrogen peroxide adduct / acetic acid / 2 h / 20 - 60 °C

With pyridine; methanol; dmap; sodium methylate; urea hydrogen peroxide adduct; In acetic acid;
DOI:10.3762/bjoc.13.113

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 869384-37-2
1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / dichloromethane / 3 h / 0 °C / Inert atmosphere

2: sodium methylate; methanol

3: pyridine; dmap / 0 °C

4: urea hydrogen peroxide adduct / acetic acid / 2 h / 20 - 60 °C

With pyridine; methanol; dmap; boron trifluoride diethyl etherate; sodium methylate; urea hydrogen peroxide adduct; In dichloromethane; acetic acid;
DOI:10.3762/bjoc.13.113

Reference yield:

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-62-0,77481-63-1,105088-17-3,149495-84-1
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 869384-37-2
1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / 0 °C

2: urea hydrogen peroxide adduct / acetic acid / 2 h / 20 - 60 °C

With pyridine; dmap; urea hydrogen peroxide adduct; In acetic acid;
DOI:10.3762/bjoc.13.113