(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate

Base Information

Chemical Name:(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate
CAS No.:1423157-23-6
Molecular Formula:C₁₉H₂₁NO₄
Molecular Weight:327.38
Hs Code.:

Synonyms:(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate

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Technology Process of (5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate

There total 2 articles about (5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1423157-28-1
(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-vinylbenzoate

: 1423157-23-6
(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate

Guidance literature:: With silver(I) nitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In 1,2-dichloro-ethane; at 70 ℃; for 12h; stereoselective reaction; Molecular sieve;
DOI:10.1021/ja311942e

Reference yield:

: 1075-49-6
4-ethenylbenzoic acid

: 308363-12-4,22567-18-6,20307-86-2
L-carveol

: 1423157-23-6
(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl 4-((E)-2-nitrovinyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C

2: silver(I) nitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / 1,2-dichloro-ethane / 12 h / 70 °C / Molecular sieve

With dmap; silver(I) nitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; dicyclohexyl-carbodiimide; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja311942e