(5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

Base Information

Chemical Name:(5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane
CAS No.:1332866-60-0
Molecular Formula:C₂₇H₅₂O₄Si₂
Molecular Weight:496.878
Hs Code.:

Synonyms:(5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

Suppliers and Price of (5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

There total 2 articles about (5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1332866-59-7
(2S,3R)-2-ethyl-5-[(4-methoxyphenyl)methoxy]pentane-1,3-diol

: 69739-34-0
t-butyldimethylsiyl triflate

: 1332866-60-0
(5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1002/hlca.201100018

Reference yield:

: (3R)-2-ethyl-3-hydroxy-5-[(4-methoxyphenyl)methoxy]-1-[(3aS,6R,7aS)-3,5,6,7-tetrahydro-8,8-dimethyl-2,2-dioxo-3a,6-methano-2,1-benzisothiazol-1(4H)-yl]pentan-1-one

: 1332866-60-0
(5R,6S)-6-ethyl-5-{2-[(4-methoxyphenyl)methoxy]ethyl}-2,2,3,3,9,9,10,10-octamethyl-4,8-dioxa-3,9-disilaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;
DOI:10.1002/hlca.201100018