(1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

Base Information

Chemical Name:(1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate
CAS No.:1304534-04-0
Molecular Formula:C₂₁H₃₀Cl₂N₂O₆
Molecular Weight:477.385
Hs Code.:

Synonyms:(1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

Chemical Property:

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Technology Process of (1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

There total 3 articles about (1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 1303598-17-5
(1R,2R)-3-(decanoyloxy)-2-[(dichloroacetyl)amino]-1-(4-nitrophenyl)propyl decanoate

: 1304534-04-0
(1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

Guidance literature:: With Novozym 435; In acetonitrile; at 20 ℃; for 24h; pH=7; regioselective reaction; aq. phosphate buffer; Enzymatic reaction;
DOI:10.1016/j.tet.2011.02.070

Reference yield:

: 10318-17-9
(1R,2R)-3-(acetyloxy)-2-[(dichloroacetyl)amino]-1-(4-nitrophenyl)propyl acetate

: 1304534-04-0
(1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

Guidance literature:: Multi-step reaction with 3 steps

1: Novozym 435 / acetonitrile / 24 h / 20 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

2: Candida antarctica lipase A preparation / 1,4-dioxane / 48 h / 30 °C / Enzymatic reaction

3: Novozym 435 / acetonitrile / 24 h / 20 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

With Novozym 435; Candida antarctica lipase A preparation; In 1,4-dioxane; acetonitrile;
DOI:10.1016/j.tet.2011.02.070

Reference yield:

: 56-75-7,85666-84-8
chloramphenicol

: 1304534-04-0
(1R,2R)-2-[(dichloroacetyl)amino]-3-hydroxy-1-(4-nitrophenyl)propyl decanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Candida antarctica lipase A preparation / 1,4-dioxane / 48 h / 30 °C / Enzymatic reaction

2: Novozym 435 / acetonitrile / 24 h / 20 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

With Candida antarctica lipase A preparation; Novozym 435; In 1,4-dioxane; acetonitrile;
DOI:10.1016/j.tet.2011.02.070