C₂₁H₂₈FNO₆

Base Information

Chemical Name:C₂₁H₂₈FNO₆
CAS No.:1620387-66-7
Molecular Formula:C₂₁H₂₈FNO₆
Molecular Weight:409.455
Hs Code.:

C<sub>21</sub>H<sub>28</sub>FNO<sub>6</sub>

Synonyms:C₂₁H₂₈FNO₆

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Chemical Property of C₂₁H₂₈FNO₆

Chemical Property:

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Technology Process of C₂₁H₂₈FNO₆

There total 7 articles about C₂₁H₂₈FNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620387-64-5
C₂₇H₃₁FN₂O₁₀S

: 1620387-66-7
C₂₁H₂₈FNO₆

Guidance literature:: With potassium carbonate; 4-t-butylbenzenethiol; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;
DOI:10.1016/j.tetlet.2014.06.063

Reference yield:

: 81887-89-0
2-hydroxycyclopentyl-1-carboxylic acid

: 1620387-66-7
C₂₁H₂₈FNO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 11 h / 20 °C

2.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C

3.1: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 0.5 h / 20 °C

4.1: n-butyllithium / tert-butyl methyl ether; hexane / 1 h / 0 °C / Inert atmosphere

4.2: 18 h / 0 °C / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

5.2: 0.5 h / 20 °C

6.1: triphenylphosphine; diethylazodicarboxylate / dichloromethane / 21 h / 20 °C

7.1: potassium carbonate; 4-t-butylbenzenethiol / N,N-dimethyl-formamide / 0.25 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; sulfur trioxide pyridine complex; potassium carbonate; caesium carbonate; triethylamine; 4-t-butylbenzenethiol; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; tert-butyl methyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; 4.1: |Horner-Wadsworth-Emmons Olefination / 4.2: |Horner-Wadsworth-Emmons Olefination / 6.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetlet.2014.06.063

Reference yield:

: 1620387-59-8
C₁₁H₁₈O₄

: 1620387-66-7
C₂₁H₂₈FNO₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C

2.1: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 0.5 h / 20 °C

3.1: n-butyllithium / tert-butyl methyl ether; hexane / 1 h / 0 °C / Inert atmosphere

3.2: 18 h / 0 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

4.2: 0.5 h / 20 °C

5.1: triphenylphosphine; diethylazodicarboxylate / dichloromethane / 21 h / 20 °C

6.1: potassium carbonate; 4-t-butylbenzenethiol / N,N-dimethyl-formamide / 0.25 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; sulfur trioxide pyridine complex; potassium carbonate; triethylamine; 4-t-butylbenzenethiol; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; tert-butyl methyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; 3.1: |Horner-Wadsworth-Emmons Olefination / 3.2: |Horner-Wadsworth-Emmons Olefination / 5.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetlet.2014.06.063