N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine

Base Information

• Chemical Name: N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine
• CAS No.: 219812-79-0
• Molecular Formula: C₁₅H₂₂N₂O₇
• Molecular Weight: 342.349

Synonyms:N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine

Chemical Property of N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine

There total 1 articles about N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine (219812-79-0)

Guidance literature:

Reference yield: 97.0%

diazodiphenylmethane (908093-98-1) + N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine (219812-79-0) → N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine diphenylmethyl ester hydrochloride

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃; for 1.5h;

DOI:10.7164/antibiotics.55.499

Reference yield:

4-(benzyloxycarbonylamino)butyric acid (5105-78-2) + N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine (219812-79-0) → (S)-3-[(2S,3R,4R,5S)-5-(4-Benzyloxycarbonylamino-butyrylamino)-2,3,4,6-tetrahydroxy-hexanoylamino]-3-phenyl-propionic acid

Guidance literature:

4-(benzyloxycarbonylamino)butyric acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In acetonitrile; at 20 ℃; for 3h;

N-[(2S,3R,4R,5S)-5-amino-2,3,4,6-tetrahydroxyhexanoyl]-β-D-phenylalanine; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.7164/antibiotics.55.322

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