(E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

Base Information

Chemical Name:(E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene
CAS No.:1313379-66-6
Molecular Formula:C₃₉H₃₉O₁₁PS
Molecular Weight:746.772
Hs Code.:

Synonyms:(E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

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Chemical Property of (E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

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Technology Process of (E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

There total 1 articles about (E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1231184-93-2
C₂₅H₂₆O₈S

: 538-60-3
dibenzyl hydrogen phosphite

: 1313379-66-6
(E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

Guidance literature:: With tetrachloromethane; dmap; N-ethyl-N,N-diisopropylamine; In acetonitrile; at -10 ℃; Inert atmosphere;
DOI:10.1021/np200104t

Reference yield: 32.0%

: 1313379-66-6
(E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

: (E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[(disodium)phosphate]-4-methoxyphenyl]ethene

Guidance literature:: (E)-1-[3',4',5'-trimethoxyphenyl]-2-[2"-[(para-toluenesulfonyl)oxy]-3"-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4"-methoxyphenyl]ethene; With trimethylsilyl bromide; In acetonitrile; at -10 ℃; for 3h; Inert atmosphere;

With sodium methylate; In methanol; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1021/np200104t

Reference yield:

: 1313379-66-6
(E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-[(para-toluenesulfonyl)oxy]-3-[([bis[(benzyl)oxy]]phosphoryl)oxy]-4-methoxyphenyl]ethene

: (E)-1-[3',4',5'-trimethoxyphenyl]-2-[2-hydroxy-3-[(disodium)phosphate]-4-methoxyphenyl]ethene

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylsilyl bromide / acetonitrile / 3 h / -10 °C / Inert atmosphere

1.2: -10 - 20 °C / Inert atmosphere

2.1: methanol; sodium hydroxide / 0.5 h / 50 °C / Microwave irradiation; Inert atmosphere; Capped vial

With methanol; trimethylsilyl bromide; sodium hydroxide; In acetonitrile;
DOI:10.1021/np200104t