C₃₄H₄₈N₂O₅Si

Base Information

Chemical Name:C₃₄H₄₈N₂O₅Si
CAS No.:141810-27-7
Molecular Formula:C₃₄H₄₈N₂O₅Si
Molecular Weight:592.851
Hs Code.:

C<sub>34</sub>H<sub>48</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₃₄H₄₈N₂O₅Si

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Chemical Property of C₃₄H₄₈N₂O₅Si

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Technology Process of C₃₄H₄₈N₂O₅Si

There total 10 articles about C₃₄H₄₈N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2552-93-4
C₂₂H₃₂N₄O

: 141810-27-7
C₃₄H₄₈N₂O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: 1 N NaOH / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 84 percent / CuCl₂ / tetrahydrofuran; H₂O / Ambient temperature; phosphate buffer pH 7

3: 71 percent / Et₃N / CH₂Cl₂ / 2.5 h / 0 °C

4: 78 percent / N-bromosuccinimide / tetrahydrofuran / 2 h / -22 °C

5: 71 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 65 h / Ambient temperature

6: 98 percent / NaBH₄ / methanol / 0.67 h / Ambient temperature

7: 100 percent / Et₃N, p-dimethylaminopyridine / CH₂Cl₂ / 22 h / Ambient temperature

8: 1) BH₃-Me₂S, 2) 3 N aq. NaOH, 31percent H₂O₂ / 1) THF, r.t., 2.5 h, 2) 80 to 90 deg C, 1 h

With dmap; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; dimethylsulfide borane complex; dihydrogen peroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88525-2

Reference yield:

: 4360-12-7
(+)-ajmaline

: 141810-27-7
C₃₄H₄₈N₂O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1: molecular sieves, H₂SO₄ / ethanol / 3 h / Heating

2: 1 N NaOH / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 84 percent / CuCl₂ / tetrahydrofuran; H₂O / Ambient temperature; phosphate buffer pH 7

4: 71 percent / Et₃N / CH₂Cl₂ / 2.5 h / 0 °C

5: 78 percent / N-bromosuccinimide / tetrahydrofuran / 2 h / -22 °C

6: 71 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 65 h / Ambient temperature

7: 98 percent / NaBH₄ / methanol / 0.67 h / Ambient temperature

8: 100 percent / Et₃N, p-dimethylaminopyridine / CH₂Cl₂ / 22 h / Ambient temperature

9: 1) BH₃-Me₂S, 2) 3 N aq. NaOH, 31percent H₂O₂ / 1) THF, r.t., 2.5 h, 2) 80 to 90 deg C, 1 h

With dmap; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; molecular sieve; dimethylsulfide borane complex; sulfuric acid; dihydrogen peroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; copper dichloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88525-2

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 141810-27-7
C₃₄H₄₈N₂O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: 1 N NaOH / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 84 percent / CuCl₂ / tetrahydrofuran; H₂O / Ambient temperature; phosphate buffer pH 7

3: 71 percent / Et₃N / CH₂Cl₂ / 2.5 h / 0 °C

4: 78 percent / N-bromosuccinimide / tetrahydrofuran / 2 h / -22 °C

5: 71 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 65 h / Ambient temperature

6: 98 percent / NaBH₄ / methanol / 0.67 h / Ambient temperature

7: 100 percent / Et₃N, p-dimethylaminopyridine / CH₂Cl₂ / 22 h / Ambient temperature

8: 1) BH₃-Me₂S, 2) 3 N aq. NaOH, 31percent H₂O₂ / 1) THF, r.t., 2.5 h, 2) 80 to 90 deg C, 1 h

With dmap; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; dimethylsulfide borane complex; dihydrogen peroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88525-2