4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester

Base Information

• Chemical Name: 4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester
• CAS No.: 126063-60-3
• Molecular Formula: C₃₂H₄₇NO₃Si
• Molecular Weight: 521.816

Synonyms:4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester

Chemical Property of 4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester

There total 10 articles about 4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2-(Dimethyl-hydrazonomethyl)-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester (1064666-73-4) → 4-(2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester (126063-60-3)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; methyl iodide; Multistep reaction; 2.) PhH;

DOI:10.1021/ja00035a041

Reference yield:

4-((S)-6-{4-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-2-{[(E)-(R)-2-methoxy-pyrrolidin-1-ylimino]-methyl}-hexyl)-benzoic acid tert-butyl ester → 4-((S)-2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester (126063-60-3)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; methyl iodide; Multistep reaction; 2.) PhH;

DOI:10.1021/ja00035a041

Reference yield:

4-((R)-6-{4-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-2-{[(E)-(S)-2-methoxy-pyrrolidin-1-ylimino]-methyl}-hexyl)-benzoic acid tert-butyl ester → 4-((R)-2-Cyano-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester (126063-60-3)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; methyl iodide; Multistep reaction; 2.) PhH;

DOI:10.1021/ja00035a041

upstream raw materials:

4-((S)-6-{4-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-2-{[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-methyl}-hexyl)-benzoic acid tert-butyl ester

4-(bromomethyl)benzoic acid 1,1-dimethylethyl ester

4-(2-(Dimethyl-hydrazonomethyl)-6-{4-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-phenyl}-hexyl)-benzoic acid tert-butyl ester

Downstream raw materials:

4-[(S)-2-Cyano-6-(4-hydroxy-phenyl)-hexyl]-benzoic acid tert-butyl ester

4-[2-Cyano-6-(4-hydroxy-phenyl)-hexyl]-benzoic acid

C₃₉H₄₁NO₄

4-[(R)-2-Cyano-6-(4-hydroxy-phenyl)-hexyl]-benzoic acid

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