N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine

Base Information

• Chemical Name: N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine
• CAS No.: 217792-92-2
• Molecular Formula: C₂₈H₄₄NO₁₀PS₂
• Molecular Weight: 649.764

Synonyms:N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine

Chemical Property of N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine

Chemical Property:

Purity/Quality:

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Technology Process of N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine

There total 1 articles about N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-Tyr-OH (3978-80-1) + bis(S-pivaloyl-2-thioethyl)-N,N-diisopropylphosphoramidite → N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine (217792-92-2)

Guidance literature:

Yield given; Multistep reaction;

DOI:10.1021/jo980437d

Reference yield: 87.0%

N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine (217792-92-2) → O--L-phosphotyrosine

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.166667h;

DOI:10.1021/jo980437d

Reference yield:

N-α-(tert-butoxycarbonyl)-O--L-phosphotyrosine (217792-92-2) → C42H63N6O11PS2*C2HF3O2

Guidance literature:

Multi-step reaction with 2 steps

1: 264 mg / N,N-diisopropyl-N-ethylamine, benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate / CH₂Cl₂ / 2 h / Ambient temperature

2: 83 percent / trifluoroacetic acid, anisole / CH₂Cl₂ / 0.25 h

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/jo980437d

upstream raw materials:

Boc-Tyr-OH

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