3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

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Chemical Name:3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide
CAS No.:1378869-36-3
Molecular Formula:C₂₄H₁₄F₈N₆O₂
Molecular Weight:570.401
Hs Code.:

Synonyms:3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

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Chemical Property of 3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

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Technology Process of 3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

There total 4 articles about 3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1161274-19-6
4-cyano-2-methylbenzoyl chloride

: 1378870-47-3
3-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

: 1378869-36-3
3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 132631-86-8
1-Methyl-3-(pentafluoroethyl)-4-(trifluoromethyl)-1H-pyrazol-5-amine

: 1378869-36-3
3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 6 h / Reflux

2: sodium hydroxide; sodium dithionite; tetrabutylammomium bromide / water; tetrahydrofuran / 2 h / 20 °C

3: pyridine / tetrahydrofuran / 20 °C

With pyridine; sodium dithionite; tetrabutylammomium bromide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 104315-28-8
5-fluoro-1-methyl-3-(1,1,2,2,2-pentafluoroethyl)-4-(trifluoromethyl)pyrazole

: 1378869-36-3
3-(4-cyano-2-methyl-benzoyl)-amino-4-cyano-N-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / dimethyl sulfoxide / 50 °C

2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 6 h / Reflux

3: sodium hydroxide; sodium dithionite; tetrabutylammomium bromide / water; tetrahydrofuran / 2 h / 20 °C

4: pyridine / tetrahydrofuran / 20 °C

With pyridine; sodium dithionite; tetrabutylammomium bromide; ammonia; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;