methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate

Base Information

• Chemical Name: methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate
• CAS No.: 1021438-19-6
• Molecular Formula: C₃₆H₄₉N₃O₈
• Molecular Weight: 651.8

Synonyms:methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate

Chemical Property of methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate

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Technology Process of methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate

There total 1 articles about methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl (2R,4S,7S)-7-cyclohexyl-20-ethoxy-22-iodo-23-methoxy-12,12-dimethyl-6,9-dioxo-3,4,6,7,8,9,12,13,14,15-decahydro-2H,11H-16,18-etheno-2,5-methanopyrido[4,3-k][1,10,3,6]dioxadiazacyclononadecine-4-carboxylate (1021438-17-4) + tri-n-butyl(vinyl)tin (7486-35-3) → methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1(23),17,19,21,24-pentaene-5-carboxylate (1021438-19-6)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 95 ℃; for 2h;

Reference yield:

methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-18-methoxy-13,13-dimethyl-7,10-dioxo-19-vinyl-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1(23),17,19,21,24-pentaene-5-carboxylate (1021438-19-6) → methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-19-ethyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1(23),17,19,21,24-pentaene-5-carboxylate (1021438-21-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 18h;

upstream raw materials:

methyl (2R,4S,7S)-7-cyclohexyl-20-ethoxy-22-iodo-23-methoxy-12,12-dimethyl-6,9-dioxo-3,4,6,7,8,9,12,13,14,15-decahydro-2H,11H-16,18-etheno-2,5-methanopyrido[4,3-k][1,10,3,6]dioxadiazacyclononadecine-4-carboxylate

tri-n-butyl(vinyl)tin

Downstream raw materials:

methyl (3R,5S,8S)-8-cyclohexyl-22-ethoxy-19-ethyl-18-methoxy-13,13-dimethyl-7,10-dioxo-2,11-dioxa-6,9,21-triazatetracyclo[15.6.2.1(3,6).0(20,24)]hexacosa-1⁽²³⁾,17,19,21,24-pentaene-5-carboxylate

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