C₅₉H₉₇N₁₅O₂₄

Base Information

Chemical Name:C₅₉H₉₇N₁₅O₂₄
CAS No.:1402052-02-1
Molecular Formula:C₅₉H₉₇N₁₅O₂₄
Molecular Weight:1400.51
Hs Code.:

C<sub>59</sub>H<sub>97</sub>N<sub>15</sub>O<sub>24</sub>

Synonyms:C₅₉H₉₇N₁₅O₂₄

Suppliers and Price of C₅₉H₉₇N₁₅O₂₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of C₅₉H₉₇N₁₅O₂₄

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₅₉H₉₇N₁₅O₂₄

There total 6 articles about C₅₉H₉₇N₁₅O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 1402051-93-7
C₂₃H₄₃N₇O₁₀

: 1402052-02-1
C₅₉H₉₇N₁₅O₂₄

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2.25h; Inert atmosphere;
DOI:10.1002/chem.201200550

Reference yield:

: 1402051-90-4
C₂₇H₄₃N₅O₈

: 1402052-02-1
C₅₉H₉₇N₁₅O₂₄

Guidance literature:: Multi-step reaction with 5 steps

1: triethylsilane / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: hydrogenchloride / water / Inert atmosphere

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2.25 h / 20 °C / Inert atmosphere

4: hydrogenchloride; 20% palladium hydroxide on charcoal; hydrogen / methanol; diethyl ether / 4 h / 20 °C

5: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2.25 h / 20 °C / Inert atmosphere

With hydrogenchloride; triethylsilane; 20% palladium hydroxide on charcoal; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201200550

Reference yield:

: C₁₇H₂₇N₅O₄*(x)ClH

: 1402052-02-1
C₅₉H₉₇N₁₅O₂₄

Guidance literature:: Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2.25 h / 20 °C / Inert atmosphere

2: hydrogenchloride; 20% palladium hydroxide on charcoal; hydrogen / methanol; diethyl ether / 4 h / 20 °C

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2.25 h / 20 °C / Inert atmosphere

With hydrogenchloride; 20% palladium hydroxide on charcoal; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/chem.201200550