1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene

Base Information

• Chemical Name: 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene
• CAS No.: 1001404-25-6
• Molecular Formula: C₁₂H₂₁N₃O₃
• Molecular Weight: 255.317
• Mol file: 1001404-25-6.mol

Synonyms:1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene

Chemical Property of 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene

There total 4 articles about 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,3,5-tri(azidomethyl)-2,4,6-trimethoxybenzene (1001404-24-5) → 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene (1001404-25-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 48h; under 36201.3 Torr;

DOI:10.1021/acs.inorgchem.1c00244

Reference yield: 83.0%

2,2′,2′′-[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(isoindoline-1,3-dione) → 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene (1001404-25-6)

Guidance literature:

With hydrazine hydrate; potassium hydroxide; In ethanol; toluene; for 20h; Reflux;

DOI:10.1039/c3ob41540f

Reference yield:

1,3,5-tris(bromomethyl)-2,4,6-(trimethoxy)benzene (434323-17-8) → 1,3,5-tris(aminomethyl)-2,4,6-trimethoxybenzene (1001404-25-6)

Guidance literature:

1,3,5-tris(bromomethyl)-2,4,6-(trimethoxy)benzene; With potassium phtalimide; In dimethyl sulfoxide; at 100 ℃; for 21h;

With hydrazine hydrate; In ethanol; toluene; for 20h; Reflux;

DOI:10.1055/s-2016-1561449

upstream raw materials:

1,3,5-tri(azidomethyl)-2,4,6-trimethoxybenzene

1,2,3-trimethoxybenzene

1,3,5-tris(bromomethyl)-2,4,6-(trimethoxy)benzene